• 电话:0531-88364464
  • 传真:0531-88564464
  • 地址:
    中国山东省济南市山大南路27号
  • 邮编:250100

导师风采

【个人简介】

占金华,男,1974年生,博士,于2000年获得中国科学技术大学化学系博士学位后,先后在台湾大学化学系、国立物质材料研究机构(NIMS)从事研究工作,2006年加入山东大学化学与化工学院. 担任化学与化工学院副院长、胶体与界面化学教育部重点实验室副主任, SCIENCECHINA Materials编委。主要从事纳米材料的表面修饰以及在难降解环境有害物快速检测与催化降解中的应用。

 承担了科技部重大研究计划(973)、国家自然科学基金等10多项科研课题的研究,2007入选教育部新世纪人才,获得山东省杰出青年基金,在AngewandteChemie等期刊发表论文140多篇,被引用5000多次,H因子41


【学习及工作经历】

  •  2001.03-2002.12 台湾大学化学系
    2003.02-2006.11 物质材料研究机构(日本)
    2006.11-至今     山东大学化学与化工学院
  •  电话:0531-8836-5017

【主讲课程】

  • 分析化学
  • 纳米材料学
  • 环境纳米材料化学

【研究领域和兴趣】

  •  1,纳米材料的可控合成以及功能调节
    2,易挥发性有机物气敏传感器与痕量有害物的表面增强拉曼光谱检测
    (与企业合作、质检机构合作)
    3,纳米材料的环境效应与污染物的催化转化(与南方环保合作)
    4,纳米材料在诊断治疗学中的应用(与齐鲁医院合作)。

【主要论著】

  • 2018

  • 1. Efficient activation of persulfate by Fe 3 O 4@β-cyclodextrin nanocomposite for removal of bisphenol A. RSCAdvances 8.27 (2018): 14879-14887.

  • 2. In-situ generation ofhighly dispersed Au nanoparticles on porous ZnO nanoplates via ion exchangefrom hydrozincite for VOCs gas sensing[J]. Sensors and Actuators B: Chemical,2018, 255: 884-890.

  • 3. Biocompatible and pH-sensitive MnO-loadedcarbonaceous nanospheres (MnO@ CNSs): A theranostic agent for magneticresonance imaging-guided photothermal therapy. Carbon (2018).

  • 4. Recyclable silvernanoplate-decorated copper membranes for solid-phase extraction coupled withsurface-enhanced Raman scattering detection. AnalyticalMethods 10.11 (2018): 1353-1361

  • 5. In 2 O 3-SnO 2 hybridporous nanostructures delivering enhanced formaldehyde sensing performance. Journal of Alloys and Compounds 746 (2018): 36-44.

  • 6. Hydrophobic W18O49mesocrystal on hydrophilic PTFE membrane as efficient solar steam generationdevice under one sun.  Journal of Materials Chemistry A 6.23 (2018): 10939-10946.

  • 7. Cu 2 O@ β-cyclodextrinas a synergistic catalyst for hydroxyl radical generation and molecularrecognitive destruction of aromatic pollutants at neutral pH. Journal ofhazardous materials (2018).

  • 2017

  • 1. Porous silver coating fiber for rapidlyscreening organotin compounds by solid phase microextraction coupled withsurface enhanced Raman spectroscopy, RSC Advances., 2017, 7, 3117-3124;

  • 2. Electrostatic-driven solid phasemicroextraction coupled with surface enhanced Raman spectroscopy for rapidanalysis of pentachlorophenol, Anal. Methods, 2017, 9, 459-464;

  • 3. Hydrophobic silver nanowire membrane for swabbing extraction and insitu SERS detection of polycyclic aromatic hydrocarbons on toys, Anal. Methods, 2017, 9, 1816-1824

  • 4. Au@Ag core–shell nanoparticles with a hiddeninternal reference promoted quantitative solid phase microextraction-surfaceenhanced Raman spectroscopy detection, RSC Adv., 2017, 7, 23866-23874

  • 5. High reliable androbust ultrathin-layer gold coating porous silver substrate via galvanic-freedeposition for solid phase microextraction coupled with surface enhanced Ramanspectroscopy[J]. Analytica Chimica Acta,2017

  • 2016

  • 1.Biocompatible caramelized carbonaceous nanospheres supported paramagnetic ultrathinmanganese oxide nanosheets via self-sacrificing reduction as a MRI contrastagent for liver imaging. Carbon. 2016

  • 2.Heteroepitaxial Growth of Well-Dispersed Co3O4 Nanocatalysts on Porous ZnONanoplates via Successive Hydrothermal Deposition. ChemNanoMat. 2016

    3.A positively charged silver nanowire membrane for rapid on-site swabbingextraction and detection of trace inorganic explosives using a portable Ramanspectrometer. J. Nano Res. (2016) 9: 2487

    4. Acetic acid inducedsynthesis of laminatedactivated carbon nitride nanostructures. Carbon 107(2016) 747-753

    5.Dimolecular interaction between graphitic carbon nitride nanosheets andphenols: A mechanism study. Carbon 102 (2016) 462-469

    6.Revealing the role of oxidation state in interaction betweennitro/amino-derived particulate matter and blood proteins. 2016;6: 25909

    7.Surface enhanced Raman spectroscopy hyphenated with surface microextraction forin-situ detection of polycyclic aromatic hydrocarbons on food contact materials.Talanta 158 (2016) 322–329

    8.Au-deposited porous single-crystalline ZnO nanoplates for gas sensing detectionof total volatile organic compounds. Rsc Advances, 2016, 6(44):37750-37756

    9.Au-coated ZnO nanorods on stainless steel fiber for self-cleaning solid phasemicroextraction-surface enhanced Raman spectroscopy. Analytica Chimica Acta 923(2016) 66-73

    10.Radar-Like MoS2 Nanoparticles as a High Efficient 808 nm Laser-InducedPhotothermal Agent for Cancer Therapy. RSC Adv, 2016, 6, 31031-31036

    11.Facile synthesis and high formaldehyde-sensing performance of NiO–SnO 2 hybridnanospheres. RSC Adv., 2016, 6, 3919-3926

    12.Sodium Diethyldithiocarbamate (DDTC) induced formation of positively chargedsilver nanoparticles for rapid in-situ identification of inorganic explosivesby surface enhanced Raman spectroscopy. RSC Adv., 2016, 6, 51823-51829

    13.Fe3O4@β-CD nanocomposite as heterogeneous Fenton-like catalyst forenhanceddegradation of 4-chlorophenol (4-CP), Applied Catalysis B,Environmental,2016.01.071


  • 2015

    1.      Hydrophobic gold nanostructuresvia electrochemical deposition for sensitive SERS detection of persistent toxicsubstances,RSC Advances,2015,5,18,13443-13450

    2.      Recent developments onnanomaterials-based optical sensors for Hg2+ detection, SCIENCE CHINA Materials,2015,58,223-240

    3.      Silver nanoplate-decoratedcopper wire for the on-site microextraction and detection of perchlorate usinga portable Raman spectrometer,Analyst,2015,140,2815-2822

    4.      Silver nanoparticles aggregateson metal fiber for solid phase microextraction-surface enhanced Ramanspectroscopy detection of polycyclic aromatic hydrocarbons,Analyst,2015,140,4668-4675

    5.      Core–shell superparamagneticFe3O4@β-CD composites for host–guest adsorption of polychlorinated biphenyls(PCBs), Journal of Colloid and Interface Science,2015,447,1-7

    6.      Nanoparticle-based screenprinting of copper zinc tin sulfide thin film as photocathode for quantum DoTsensitized solar cell, Materials Letters,2015,158,198-201

  •  

    2014

    1. A disordered silver nanowires membranefor extraction and surface-enhanced Raman spectroscopy detection, Analyst,2014,139, 2525-2530

    2.  Galvanicdisplacement induced reduction of graphene oxide, Carbon, 2014, 66, 738-741

    3. The fabrication of oriented ZnO porousnanoplates on the silver foil with tunable hydrophobicity, CrystEngComm, 2014,16, 1831-1836

    4. Forming Buried Junctions to Enhance thePhotovoltage Generated by Cuprous Oxide in Aqueous Solutions, Angewandte Chemie,2014,53,3493-3497

    5. Tunable SERS-Tags-Hidden Gold Nanorattlesfor Theranosis of Cancer Cells with Single Laser Beam, Scientific Reports,2014,4,6709-6716

    6.  TheoreticalStudy of the Inclusion Complexation of TCDD with Cucurbit[n]urils, RSC Advances,2014,4(94)

    7. Anti-TROP2 conjugated hollow goldnanospheres as a novel nanostructure for targeted photothermal destruction ofcervical cancer cells, Nanotechnology,2014, 25(34):345103

    2013

    1.      Combination of Solid Phase Extraction and Surface-enhanced Raman Spectroscopy for Rapid, Analysis;  2013, 138, 2598-2603

    2.      Silver nanoparticles decorated filter paper via self-sacrificing reduction for membrane extraction surface-enhanced Raman spectroscopy detection; Analyst, 2013, 138, 2090-5

    3.      Electrospun porous CuO-Ag nanofibers for quantitative sensitive SERS detectionCrystEngComm2013, 15, 1339-1344

    4.      Cysteamine-Modified Silver Nanoparticle Aggregates for Quantitative SERS Sensing of Pentachlorophenol with a Portable Raman Spectrometer ACS APPLIED MATERIALS & INTERFACES, 2013, 5, 6902-6908   

    5.      Chengbu Liu New Insight into the Formation Mechanism of PCDD/Fs from 2-Chlorophenol Precursor ENVIRONMENTAL SCIENCE & TECHNOLOGY, 2013,  47, 8489-8498

    6.      Solar Hydrogen Generation by Silicon Nanowires Modified with Platinum Nanoparticle Catalysts by Atomic Layer DepositionAngewandte ChemieVolume 125Issue 42Pages 11325-11329October 112013

    7.   Surface-enhanced Raman spectroscopy detection of polybrominated diphenylethers using a portable Raman spectrometer, TALANTA, 2013, 116, 14-17

  •  

    2012

    1.      Synthesis of a beta-cyclodextrin-modified Ag film by the galvanic displacement on copper foil for SERS detection of PCBsJOURNAL OF COLLOID AND INTERFACE SCIENCE,第365卷,第1期,122-126页,2012

    2.      Porous Copper Zinc Tin Sulfide Thin Film as Photocathode for Double Junction Photoelectrochemical Solar CellCHEMICAL COMMUNICATIONS,第48卷,第24期,3006-3008页,2012

    3.      A colorimetric and Surface-enhanced Raman scattering dual-signal sensor for Hg2+ based on Bismuthiol II-capped gold nanoparticlesANALYTICA CHIMICA ACTA,第723卷,88-93页,2012

    4.    Phase Selective Synthesis of Metastable Orthorhombic Cu2ZnSnS4JOURNAL OF MATERIALS CHEMISTRY,第22卷,第15期,7502-7506页,2012

    5.      Silver nanoparticle aggregates on copper foil for reliable quantitative SERS analysis of polycyclic aromatic hydrocarbons with a portable Raman spectrometerANALYST,第137卷,第17期,3995-4000页,2012

    6.    Magnetic nanoparticles and quantum dots co-loaded imprinted matrix for pentachlorophenolJournal of Hazardous Materials,第63卷,第70期,237– 238页,2012

    7.      In situ fabrication of single-crystalline porous ZnO nanoplates on zinc foil to support silver nanoparticles as a stable SERS substrateCrystEngComm,第14卷,,18,6023–6028页,2012

  • 2011

    1.      Porous SnO2 nanospheres as sensitive gas sensors for volatile organic compounds detection Nanoscale,2011, : 3 : 4 : 1646-1652

    2.      InO2 microbundles constructed with well-aligned single-crystalline nanorods: F127-directed self-assembly and enhanced gas sensing performance; Journal of Colloid and Interface Science,Volume 354,Issue 1,2011,Pages 89-93

    3.      Facile synthesis of N-acetyl-l-cysteine capped ZnS quantum dots as aneco-friendly fluorescence sensor for Hg2+ ;Talanta ,85 , 1738– 1743,2011

    4.      Theoretical evaluation of the configurations and Raman spectra of 209polychlorinated biphenyl congeners;Chemosphere ,85 , 412–417,2011

    5.      Silver nanoplates prepared by modified galvanic displacement for surface-enhanced Raman spectroscopy;Nanoscale, 3, 2134;2011

  • 2010

    1.      Determination of Pentachlorophenol at Carbon Nanotubes Modified Electrode Incorporated with beta-Cyclodextrin 来源出版物: JOURNAL OF NANOSCIENCE AND NANOTECHNOLOGY : 10 : 11 特刊: Sp. Iss. SI : 7654-7657 出版年: NOV 2010

    2.      Aqueous Synthesis of Highly Luminescent Amorphous CdSe Quantum Dots at Low Temperature 来源出版物: CHEMISTRY LETTERS : 39 : 9 : 942-943 出版年: SEP 5 2010

    3.       Ethanol-thermal synthesis of Cd1-xZnxS nanoparticles with enhanced photodegradation of 4-chlorophenol 来源出版物: MATERIALS RESEARCH BULLETIN : 45 : 10 : 1396-1400 出版年: OCT 2010

    4.      Morphology-Dependent Gas-Sensing Properties of ZnO Nanostructures for Chlorophenol来源出版物: CHEMISTRY-AN ASIAN JOURNAL : 5: 8 : 1854-1859 出版年:2010

    5.      In2O3 Nanofibers and Nanoribbons: Preparation by Electrospinning and Their Formaldehyde Gas-Sensing Properties来源出版物: EUROPEAN JOURNAL OF INORGANIC CHEMISTRY : 21 : 3348-3353 出版年: JUL 2010

    6.      Band-gap tunable (Cu2Sn)(x/3)Zn1-xS nanoparticles for solar cells.来源出版物: CHEMICAL COMMUNICATIONS : 46 : 31 : 5749-5751 出版年:2010

    7.      One-pot Microwave Assisted Synthesis of Homogeneously Alloyed CdSexTe1-x Nanocrystals with Tunable Photoluminescence 来源出版物: MATERIALS LETTERS : 64 : 16 : 1843-1845 出版年: AUG 31 2010

    8.      One-Pot Green Synthesis and Bioapplication of l-Arginine-Capped Superparamagnetic Fe3O4 Nanoparticles .NANOSCALE RESEARCH LETTERS 5 .2 .302-307 .:FEB 2010

    9.      Monodispersed cation-disordered cubic AgInS2 nanocrystals with enhanced fluorescence .APPLIED PHYSICS LETTERS : 96 : 1 文献编号: 013104 . JAN 4 2010

  • 2009

    1.      Dmitri Golberg Synthesis of metal-semiconductor heterojunctions inside carbon nanotubes JOURNAL OF MATERIALS CHEMISTRY 2009, 19, 4414-4420

    2.    Catanionic-surfactant-controlled morphosynthesis and gas-sensing properties of corundum-type In2O3, NANOTECHNOLOGY 2009, 20, 285501

    3.      Synthesis of Starch-Stabilized Ag Nanoparticles and Hg2+ Recognition in Aqueous Media, Nanoscale Research Letters

    4.      One-Dimensional CdS/alpha-Fe2O3 and CdS/Fe3O4 Heterostructures: Epitaxial and Nonepitaxial Growth and Photocatalytic Activity Journal of Physical Chemistry C, 2009;113(32):14119-14125

    5.      Synthesis, Optical Properties, and Photocatalytic Activity of One-Dimensional CdS@ZnS Core-Shell Nanocomposites, Nanoscale Research Letters 2009,4, 558-564

    6.      Electroless Plating of Nickel Nanoparticles on CdS Nanowires, Eur. J. Inorg. Chem. 2009, 897–902

    7.      One-Pot Synthesis of Highly Luminescent CdTe Quantum Dots by Microwave Irradiation Reduction and Their Hg2+-Sensitive Properties, Nano Research 2009, 2, 67-76

  • 2008

    1.     Fabrication and Gas-Sensing Properties of Porous ZnO Nanoplates, Advanced Materials 2008, 20, 4547–4551

    2.      Ga-Doped ZnS Nanowires as Precursors for ZnO/ZnGa2O4 Nanotubes, Adv. Mater. 2008, 20, 810–814

    3.       Unconventional Ribbon-Shaped Ga2O3 Tubes with Mobile Sn Nanowire Fillings, ACS Nano 2008, 2, 107–112.

    4.      Synthesis, Structure, and Multiply Enhanced Field-Emission Properties of Branched ZnS Nanotube-In Nanowire Core-Shell Heterostructures, ACS Nano 2008, 2, 1015–1021.

  • 2007

    1.      Mg3N2-Ga: Nanoscale Semiconductor–Liquid Metal Heterojunctions inside Graphitic Carbon Nanotubes, Adv. Mater. 2007, 19, 1342–1346

    2.      High-Yield Synthesis of Rhombohedral BN Triangular Nanoplates, Advanced Materials 2007, 19, 2141-2144.

  • 2006

    1.        Hollow and Polygonous Microtubes of Mono-Crystalline Indium Germanate. Angewandte Chemie International Edition 2006, 2, 228-231  

    3.       Fabrication of ZnO nanoplate-nanorod junctions. Small 2006, 2, 62-65.

    4.       Nanofabrication on ZnO nanowires, Applied Physics Letters 2006, 89, 243111.

    5.       Carbon Nanotubes as Nanoreactors for Fabrication of Single-Crystalline Mg3N2 Nanowires, Nano Letters 2006, 61136-140

    6.       Dmitri Golberg Twinning in ultrathin silicon nanowiresInternational Journal of Materials Research-Zeitschrift für Metallkunde, 2006, 513-516 (invited paper in the special issue for Professor Aldinger).

    7.        Silica fibers with triangular cross sections, Advanced Materials, 2006, 18, 1852.

    8.        Tapered carbon nanotubes from activated carbon powders,Advanced Materials, 2006, 18, 197-200

  • 2005

    1.       Fabrication of Metal–Semiconductor Nanowire Heterojunctions, Angewandte Chemie International Edition 2005, 44, 2140-2144

    2.        Single-Catalyst Confined Growth of ZnS/Si Composite Nanowires,Advanced Materials 2005, 17, 225-230.

    3.        Biomimetic Formation of Hydroxyapatite Nanorods by a Single-Crystal-to-Single-Crystal Transformation, Advanced Functional Materials 2005, 15, 2005-2010

    4.        Unconventional Gallium Oxide Nanowires, Small 2005, 1, 883-888

    5.        Liquid Gallium Columns Sheathed with Carbon: Bulk Synthesis and Manipulation, Journal of the Physical Chemistry B 2005, 109, 11580-11584.

    6.        Synthesis and microstructure of Cd4SiS6/Si composite nanowires, Journal of Electron Microscopy, 2005, 54, 485-491 (invited paper in memory of the late Professor John M. Cowley)

    7.      Uniform and high-quality submicrometer tubes of GaS layered crystals,  Applied Physics Letters 2005, 87, 153112.

    8.       A Liquid-Ga-Filled Carbon Nanotube: A Miniaturized Temperature Sensor and Electrical SwitchSmall 2005, 1, 1088-1093

    9.       Single-crystalline nanotubes of IIB-VI semiconductorsApplied Physics Letters 2005, 87, 113107.

    10.    Fabrication of Silica-Shielded Ga-ZnS metal-Semiconductor Nanowire heterojunctionsAdvanced Materials 2005, 17, 1964-1969

    11.    A ssembled Highly Faceted Wurtzite-Type ZnS Single-Crystalline Nanotubes with Hexagonal Cross-Sections Advanced Materials 2005, 17 1972-1977

    12.   Growth of wurtzite ZnS micrometer-sized diskettes and nanoribbon arrays with improved luminescenceAdvanced Functional Materials 2005, 15, 757-762

    13.   Self-assembly of SiO2 nanowires and Si microwires into hierarchical heterostructures on a large scale Advanced Materials 2005, 17, 971-975.

    14.   Single-crystalline, submicrometer-sized ZnSe tubes,Advanced Materials 2005, 17, 975-979

  • 2004

    1.        Synthesis and field-emission properties of Ga2O3-C nanocables,Chemistry of Materials 2004, 16, 5158-5161.

    2.       Bulk Synthesis of Single-Crystalline Magnesium Oxide Nanotubes, Inorganic Chemistry 2004, 43, 2462-2464.

    3.      Fabrication of ZnS/SiC nanocables, SiC-shelled ZnS nanoribbons (and sheets), and SiC nanotubes (and tubes), Applied Physics Letters 2004, 85, 2932-2934.

    4.      Si/ZnS and Si/ZnSe core/shell nanocrystal structures, Applied Physics Letters2004, 85, 3593-3595.

    5.      Sn-filled single-crystalline Wurtzite-type ZnS nanotubes, Angewandte Chemie International Edition 2004, 43, 4606-4609.

    6.       Growth of single-crystalline cubic GaN nanotubes with rectangular cross sections, Advanced Materials 2004, 16, 1465-1468.

    7.     Unusual freezing and melting of gallium encapsulated in carbon nanotubes, Physical Review Letters 2004, 93, 095504-1-4

    8.      High resolution P-31 NMR study of octacalcium phosphate,Solid State Nuclear Magnetic Resonance 2004, 26, 99-104.

    9.      The first template-free growth of crystalline silicon microtubes,Advanced Functional Materials 2004, 16, 610-614.

    10. Growth and field-emission properties of crystalline, thin-walled carbon microtubes, Advanced Materials 2004, 16, 153-156.

    11.   Two-dimensional extremely thin single-crystalline alpha-Si3N4microribbons, Applied Physics Letters 2004, 84, 804-806.

    12.   Synthesis of crystalline silicon tubular nanostructures with ZnS nanowires as removable templates, Angewandte Chemie International Edition 2004, 43, 63-66.

  • 2003

    1.     Biomimetic formation of porous single-crystalline CaCO3 via nanocrystal aggregation,Advanced Materials 2003, 15, 621-623.

    2.      Epitaxial heterostructures: Side-to-side Si-ZnS, Si-ZnSe biaxial nanowires, and sandwichlike ZnS-Si-ZnS triaxial nanowires, Journal of the American Chemical Society 2003, 125, 11306-11313.

    3.    Two-dimensional micrometer-sized single-crystalline ZnO thin nanosheets, Applied Physics Letters 2003, 83, 4414-4416.

     

     

     

 

 

 

 

 

 

 



【科研项目】

1)国家自然科学基金 ;2015
2)  国家科技部重大研究计划 “973”项目课题;2014
4)国家自然科学基金面上项目;2010-2012
5)国家自然科学基金重大研究计划;2011-2013
6)国家自然科学基金;2011-2013
7)山东省自然科学基金杰出青年项目;2011-2013
8)山东大学自主创新基金-杰出青年培育项目;2010-2012

【科研成果】

【所获专利】

 

一种氧化铟纳米线聚集体的制备方法(200710114642.4)

 

一维CdS/TiO2复合半导体光催化纳米材料及其制备方法(200710116037.0)

 

片状多孔结构的ZnO纳米粉体的制备方法(200710114004.2)

 

一维CdS-Ni 半导体-磁性功能复合纳米材料及其制备方法(200710114838.3)

 

SiO2/TiO2空心复合结构材料及其制备方法与应用(200710116036.6)

 

一种超顺磁四氧化三铁纳米粒子的制备方法(200910015366.5)

 

Ca-Bi-O系可见光光催化材料及其制备方法(200910016262.6)

 

一种以表面覆盖银纳米结构的铜粉为填料的导电浆料的制备方法(201010197864.9)

 

一种在铜材料上覆盖银纳米片的方法(201010115658.9)

 

可图案化环境催化材料及其浆料的制备(201210278777.6)

 

一种水相合成铜锌锡硒纳米颗粒的制备方法(201110094002.8)

 

可调禁带宽度的Cu-Sn-Zn-S半导体材料及其制备方法(201010121968.1)

【联合培养情况】

与美国、日本、澳大利亚等多个研究小组保持着长期的合作关系,并聘请了美国加州大学的Yadong Yin教授、王敦伟教授,日本的Yoshio Bando教授等人为本实验室的合作指导教师,学生可以根据实际情况前往合作研究、联合培养或者继续深造。 

【拟招收研究生情况】

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